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- W2006331326 abstract "Abstract One of the known methods for producing bis (fluorosulfuryl) peroxide is electrolysis under vacuum at about −23°C of a dilute solution of potassium fluorosulfate in fluorosulfuric acid. This process has now been improved by increasing the concentration of the dissolved salt, thereby increasing the electrical conductivity and lowering the vapor pressure of the electrolyte. Both the rate and the current efficiency of production of S 2 O 6 F 2 have been increased and loss of HSO 3 F by evaporation has been reduced. A current efficiency of about 92% has been found for a cell operating at about −8°C with platinum electrodes in an electrolyte containing about three moles of HSO 3 F per mole of KSO 3 F. Potassium fluorosulfate combines with fluorosulfuric acid to form the compound, KSO 3 F. 3HSO 3 F, which melts at −10°C. The formation of compounds having compositions KSO 3 F. xHSO 3 F (x=3−5)are also indicated and will be discussed." @default.
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- W2006331326 date "1982-09-01" @default.
- W2006331326 modified "2023-09-24" @default.
- W2006331326 title "Electrolytic preparation of bis(fluorosulfuryl) peroxide" @default.
- W2006331326 doi "https://doi.org/10.1016/s0022-1139(00)85391-9" @default.
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