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- W2006357612 abstract "Perfluoroalkylated glycerol (5, 9) and crown ethers (22, 23, 24) were synthesized starting from glycerol. 5 was synthesized by allylation of glycerol 1,2-acetonide followed by perfluoroalkylation initiated with sodium dithionite, reduction of iodide and hydrolysis in good overall yield and was shown to possess good surface activities. Glycerol bis-ether (9) was synthesized in a similar way. Allyloxymethyl crown ethers (15, 16, 18) were prepared as key intermediates through multi-step reactions, which were then perfluoroalkylated to give the title crown ethers 33, 33, 34." @default.
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- W2006357612 date "2010-08-27" @default.
- W2006357612 modified "2023-09-24" @default.
- W2006357612 title "Synthesis of polyfluoroalkylated glycerol and crown ether" @default.
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- W2006357612 doi "https://doi.org/10.1002/cjoc.19950130310" @default.
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