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- W2006365326 abstract "Abstract Some dithioxophosphoranes 3 stabilized by intramolecular coordination with a dialkylamino group were prepared, and their structures were analyzed by X‐ray crystallography involving [2,4‐di‐ tert ‐butyl‐6‐(isopropylmethylamino)phenyl]‐ ( 3c ), {2,4‐di‐ tert ‐butyl‐6‐[(dimethylamino)methyl]phenyl}‐ ( 3f ), and {2,4‐di‐ tert ‐butyl‐6‐[2‐(dimethylamino)‐1,1‐dimethylethyl]phenyl}dithioxophosphorane ( 3h ). The bond between the phosphorus atom and the aromatic ring is flexible and the angle narrows with decreasing ring size of the intramolecular coordination. The 31 P‐NMR signals are shifted to higher field with increasing ring size of the intramolecular coordination or strength of coordination. Similarly, the corresponding diselenoxophosphoranes 4 were prepared. Both their 31 P‐ and 77 Se‐NMR signals are shifted to higher field with increasing contribution of intramolecular coordination." @default.
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- W2006365326 date "1996-09-01" @default.
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- W2006365326 title "Preparation and Structure of Dithioxo‐ and Diselenoxophosphoranes Stabilized by Intramolecular Coordination with a Dialkylamino Group" @default.
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- W2006365326 doi "https://doi.org/10.1002/cber.19961290912" @default.
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