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• W2006456084 abstract "Mandelic acid, a key precursor of chiral synthons, was successfully acylated in diisopropyl ether. The reaction was catalyzed by the lipase from Pseudomonas stutzeri LC2-8, and vinyl acetate was employed as acyl donor. Under the optimized reaction conditions, a resolution of 180 mM (55 g/L) mandelic acid was achieved. (S)-O-Acetyl mandelic acid was enantioselectivity formed in >99% ee at a yield close to the maximum theoretical value for kinetic resolution (50%). The highly substrate tolerable and enantioselective nature of lipase LC2-8 suggests that it is of great potential for the practical resolution of racemic mandelic acid. Additionally, the high enantiopreference of lipase LC2-8 toward (S)-mandelic acid in acetylation was also rationalized through molecular docking and molecular dynamics simulations." @default.
• W2006456084 created "2016-06-24" @default.
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• W2006456084 date "2014-01-01" @default.
• W2006456084 modified "2023-10-10" @default.
• W2006456084 title "Highly efficient resolution of mandelic acid using lipase from Pseudomonas stutzeri LC2-8 and a molecular modeling approach to rationalize its enantioselectivity" @default.
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• W2006456084 doi "https://doi.org/10.1016/j.molcatb.2013.10.026" @default.
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