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• W2006468237 abstract "The aminocarbyne complex Cp∗(CO)2W≡CNEt2 (Cp∗ = C5Me5) (1) undergoes a selective [2 + 2] cycloaddition reaction with the nitrilium salt [MeC≡NMe]B4 to afford the iminocarbene complex [Cp∗(CO)2W{ = C(NEt2)C(Me) = NMe}]BF4 (2). Alternatively, the analogous iminocarbene complexes [Cp∗(CO)2W{ = C(NMe2)C(Me) = NEt}]BF4 (5: M = Mo; 6: M = W) can be obtained by methylation of the η2-1,4-diaza-3-methylbutadien-2-yl complexes Cp∗(CO)2M[C(NMe)C(Me)NEt] (3: M = Mo; 4: M = W) with [Me3O]BF4. The solid-state structure of 2 suggests the presence of an η3-bonded iminocarbene ligand and reveals a close electronic relationship between 2, 5 and 6 and MoII or WII η3-vinylcarbene complexes." @default.
• W2006468237 created "2016-06-24" @default.
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• W2006468237 date "1995-10-01" @default.
• W2006468237 modified "2023-09-27" @default.
• W2006468237 title "Metal-carbon multiple bonds: [2 + 2] cycloaddition of nitrilium salts across a metal-carbon triple bond; synthesis and structure of iminocarbene complexes of tungsten" @default.
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• W2006468237 doi "https://doi.org/10.1016/0022-328x(95)05768-k" @default.
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