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- W2006536854 abstract "Abstract The i.r. spectra of the title compounds were recorded between 4000 and 200 cm −1 as melts and as polycrystalline solids between CsI plates. Pellets in KI and polyethylene matrices were studied in the regions 4000-200 and 500-30 cm −1 , respectively. Raman spectra of the compounds as crystalline solids were obtained, 3,3′-dibromobiphenyl was also studied as a melt, whereas 3,5,4′-tribromobiphenyl was investigated as a solute in CS 2 and C 6 H 6 . solutions. The spectra indicate that the three brominated biphenyls are nonplanar in the melt, in solution and in the crystalline state, as independently observed in the vapour phase by electron diffraction technique. A few i.r. and Raman bands observed in the melt and in solution of 3,3′-dibromobiphenyl, vanishing in the crystal spectra, may suggest a second conformer in the melt. Force constant calculations have been carried out, adopting a simple valence force field derived for condensed aromatics and previously applied to biphenyl. Tentative assignments of practically all the fundamentals in the title compounds were made, based upon the Raman polarization measurements, i.r. dichroism and the results of the force constant calculations." @default.
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- W2006536854 date "1985-01-01" @default.
- W2006536854 modified "2023-09-26" @default.
- W2006536854 title "The vibrational spectra and molecular structure of 3,3′-dibromo-, 3,5,4′-tribromo- and 3,5,3′,5′-tetrabromobiphenyl" @default.
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- W2006536854 doi "https://doi.org/10.1016/0584-8539(85)80150-1" @default.
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