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• W2006541310 abstract "The adsorption of sulfate or OH species and subsequent Ni(OH)2 film growth on Ni(1 1 1) single crystal electrodes has been investigated using in situ infrared reflection absorption spectroscopy (IRAS) as well as scanning tunneling microscopy (STM). In a pH 3 sulfuric acid solution, STM images show that a well-defined Ni(1 1 1) surface with a (1 × 1) lattice is exposed at −300 mV, while hexagonal close-packed images with an atomic spacing of 0.32 nm are grown on this electrode at 300 mV. On the other hand, IRAS results in a sulfuric acid solution (pH 3) reveal that an absorption band at 1116 cm−1, which can be ascribed to ν(S–O) symmetric stretching of sulfate anion on Ni(1 1 1) surface, starts to appear at −400 mV and develops its intensity with an electrode potential increase, while an absorption band at 930 cm−1 begins to develop at 0 mV on Ni(1 1 1), Ni(1 0 0) and Ni(1 1 0) electrodes, which can be assigned to an in-plane δ(Ni–OH) bending vibration in Ni(OH)2 passive film." @default.
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• W2006541310 date "2004-05-01" @default.
• W2006541310 modified "2023-10-10" @default.
• W2006541310 title "Surface structures at the initial stages in passive film formation on Ni(111) electrodes in acidic electrolytes" @default.
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• W2006541310 doi "https://doi.org/10.1016/j.jelechem.2003.11.050" @default.
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