Matches in SemOpenAlex for { <https://semopenalex.org/work/W2006556369> ?p ?o ?g. }
Showing items 1 to 87 of
87
with 100 items per page.
- W2006556369 endingPage "82" @default.
- W2006556369 startingPage "75" @default.
- W2006556369 abstract "A procedure for the determination of acetaldehyde, acetone, methanol, ethanol, 1-propanol and 2-propanol in blood was developed. Separation of analytes was carried out on DB-wax capillary column (l = 30 m, I.D. = 0.32 mm, dF = 0.5 microm) at 40 degrees C, hydrogen was used as a carrier gas (at 30 kPa) and FID as a detector. Quantification was performed with the use of 2-butanol as an internal standard. Headspace solid-phase microextraction was applied as the sample preparation technique. The usefulness of most commercially available fiber coatings was checked and 65 microm Carbowax/DVB proved most effective. Microextraction was carried out from the headspace at 60 degrees C for 10 min. The sample was stirred at 750 rpm. In order to improve the extraction efficiency of analytes, salting-out agents were also applied. Potassium carbonate turned out to be the most efficient. A 1.0-g amount of this salt and 0.1 ml of I.S. were added to 0.5 ml of sample. Validation of the worked-out method was performed. For each analyte, the limits of detection and quantification, linearity, working range, accuracy and precision were determined or tested." @default.
- W2006556369 created "2016-06-24" @default.
- W2006556369 creator A5081375577 @default.
- W2006556369 creator A5083033375 @default.
- W2006556369 creator A5065008828 @default.
- W2006556369 date "2002-06-01" @default.
- W2006556369 modified "2023-10-16" @default.
- W2006556369 title "Optimization of solid-phase microextraction conditions for gas chromatographic determination of ethanol and other volatile compounds in blood" @default.
- W2006556369 cites W2003033181 @default.
- W2006556369 cites W2015981001 @default.
- W2006556369 cites W2047323788 @default.
- W2006556369 cites W2048915458 @default.
- W2006556369 cites W2086349245 @default.
- W2006556369 cites W2090495391 @default.
- W2006556369 cites W2104291200 @default.
- W2006556369 doi "https://doi.org/10.1016/s1570-0232(02)00143-5" @default.
- W2006556369 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/12015272" @default.
- W2006556369 hasPublicationYear "2002" @default.
- W2006556369 type Work @default.
- W2006556369 sameAs 2006556369 @default.
- W2006556369 citedByCount "52" @default.
- W2006556369 countsByYear W20065563692012 @default.
- W2006556369 countsByYear W20065563692013 @default.
- W2006556369 countsByYear W20065563692014 @default.
- W2006556369 countsByYear W20065563692015 @default.
- W2006556369 countsByYear W20065563692016 @default.
- W2006556369 countsByYear W20065563692017 @default.
- W2006556369 countsByYear W20065563692019 @default.
- W2006556369 countsByYear W20065563692020 @default.
- W2006556369 countsByYear W20065563692021 @default.
- W2006556369 countsByYear W20065563692022 @default.
- W2006556369 crossrefType "journal-article" @default.
- W2006556369 hasAuthorship W2006556369A5065008828 @default.
- W2006556369 hasAuthorship W2006556369A5081375577 @default.
- W2006556369 hasAuthorship W2006556369A5083033375 @default.
- W2006556369 hasConcept C10390740 @default.
- W2006556369 hasConcept C113196181 @default.
- W2006556369 hasConcept C119128265 @default.
- W2006556369 hasConcept C123460561 @default.
- W2006556369 hasConcept C162356407 @default.
- W2006556369 hasConcept C178790620 @default.
- W2006556369 hasConcept C185592680 @default.
- W2006556369 hasConcept C205345274 @default.
- W2006556369 hasConcept C2778292535 @default.
- W2006556369 hasConcept C2778533135 @default.
- W2006556369 hasConcept C2778576202 @default.
- W2006556369 hasConcept C2779607525 @default.
- W2006556369 hasConcept C2781213060 @default.
- W2006556369 hasConcept C43617362 @default.
- W2006556369 hasConcept C4725764 @default.
- W2006556369 hasConceptScore W2006556369C10390740 @default.
- W2006556369 hasConceptScore W2006556369C113196181 @default.
- W2006556369 hasConceptScore W2006556369C119128265 @default.
- W2006556369 hasConceptScore W2006556369C123460561 @default.
- W2006556369 hasConceptScore W2006556369C162356407 @default.
- W2006556369 hasConceptScore W2006556369C178790620 @default.
- W2006556369 hasConceptScore W2006556369C185592680 @default.
- W2006556369 hasConceptScore W2006556369C205345274 @default.
- W2006556369 hasConceptScore W2006556369C2778292535 @default.
- W2006556369 hasConceptScore W2006556369C2778533135 @default.
- W2006556369 hasConceptScore W2006556369C2778576202 @default.
- W2006556369 hasConceptScore W2006556369C2779607525 @default.
- W2006556369 hasConceptScore W2006556369C2781213060 @default.
- W2006556369 hasConceptScore W2006556369C43617362 @default.
- W2006556369 hasConceptScore W2006556369C4725764 @default.
- W2006556369 hasIssue "1" @default.
- W2006556369 hasLocation W20065563691 @default.
- W2006556369 hasLocation W20065563692 @default.
- W2006556369 hasOpenAccess W2006556369 @default.
- W2006556369 hasPrimaryLocation W20065563691 @default.
- W2006556369 hasRelatedWork W2033042113 @default.
- W2006556369 hasRelatedWork W2079128366 @default.
- W2006556369 hasRelatedWork W2097259216 @default.
- W2006556369 hasRelatedWork W2979490278 @default.
- W2006556369 hasRelatedWork W3082649180 @default.
- W2006556369 hasRelatedWork W4210312647 @default.
- W2006556369 hasRelatedWork W4385413829 @default.
- W2006556369 hasRelatedWork W4387264802 @default.
- W2006556369 hasRelatedWork W902063304 @default.
- W2006556369 hasRelatedWork W2297486106 @default.
- W2006556369 hasVolume "773" @default.
- W2006556369 isParatext "false" @default.
- W2006556369 isRetracted "false" @default.
- W2006556369 magId "2006556369" @default.
- W2006556369 workType "article" @default.