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- W2006561693 abstract "Under low energy sputtering conditions (e.g. Ar+ ions, 300 eV, 10−8A cm−2) the Secondary Ion Mass Spectra show almost only those polyatomic ions which correspond to the arrangement of the atoms in the crystal structure. This method for obtaining structural information is demonstrated on a single crystal of cubic ZnS. In the SIMS for this pure ZnS crystal mainly polyatomic ions such as (ZnS)+, (ZnS)−, (ZnSZn)+, (SZnS)−, etc. were observed. Other polyatomic ions such as (Zn2)+ or (S2−), which are not originally present in the crystal, are observed only in a very low counting rate ratio. An increase in the energy of the primary ions causes larger clusters of atoms of the crystal to be taken off, as well as polyatomic ions which do not correspond to the original structure. These effects and the influence of the crystallographic orientations are demonstrated on single crystals of CaF2. Two applications of this method are discussed: the determination of S2 content in thin films of ZnS and the identification of “FeAl2O4” clusters in activated ammonia catalysts (α-Fe+ 3%Al2O3)." @default.
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- W2006561693 date "1975-01-01" @default.
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- W2006561693 title "Crystal structures and their secondary ion mass spectra" @default.
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- W2006561693 doi "https://doi.org/10.1016/0039-6028(75)90299-x" @default.
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