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- W2006571835 abstract "A new aluminophosphate compound |(CH2)6N4H3·H2O|[Al11P12O48] (denoted AlPO-CJB2) with a three-dimensional open framework and an Al/P ratio of 11/12 has been synthesized solvothermally by using hexamethylenetetramine as a template. It was characterized by X-ray powder diffraction, inductively coupled plasma, elemental (CHN), and thermogravimetric analyses, and the structure was determined by single-crystal X-ray diffraction analysis. AlPO-CJB2 crystallizes in the trigonal space group R-3c with a=14.088(2) Å, c=42.199(9) Å, and Z=6. Its structure features two new kinds of cages, i.e., cage 1, 412436686 and cage 2, 412612. The two cages alternate along the [0 0 1] direction forming an infinite column by sharing a common snowflake-like chiral motif, which is constructed from an AlO6-centered six four-membered rings. The title compound is constructed from strictly alternating Al polyhedra (AlO4 and AlO6) and P tetrahedra (PO4) via bridging oxygen atoms, and presents a new type of stoichiometry with an Al/P ratio of 11/12 in the aluminophosphate family. Computer simulation was used to determine the possible positions of the organic template within the cages." @default.
- W2006571835 created "2016-06-24" @default.
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- W2006571835 date "2001-12-01" @default.
- W2006571835 modified "2023-10-18" @default.
- W2006571835 title "An anionic framework aluminophosphate |(CH2)6N4H3·H2O|[Al11P12O48] and computer simulation of the template positions" @default.
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- W2006571835 doi "https://doi.org/10.1016/s1387-1811(01)00442-5" @default.
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