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• W2006603728 abstract "Abstract A new method through intercalation and exfoliation of VOPO4·2H2O crystallites in primary alcohol (1-propanol or 1-butanol), followed by reduction with the alcohol, have been investigated for the preparation of catalyst precursor. Lamellar compounds, consisting of V4+, P5+ and alkyl group with thin film-like morphology, were formed and was characterized by means of XRD, IR, TG/DTA, and elemental analysis. The chemical formula of the precursor obtained by exfoliation–reduction in 1-butanol was shown to be VO{(n-C4H9)0.16H0.84}PO4·0.8H2O. On the other hand, a direct reduction of VOPO4·2H2O in the alcohol gave a mixed phase shown by (VOHPO4·0.5H2O)0.3(VO{(n-C4H9)0.3H0.7}PO4·3H2O)0.7 comprising plate-like microcrystallites. These precursors transformed to (VO)2P2O7 phase during an activation process at 703 K in the presence of a mixture of n-butane 1.5% and O2 17% in He balance. The obtained (VO)2P2O7 through the exfoliation–reduction was well crystallized and consisted of thin flaky crystallites. It was found that (VO)2P2O7 thus prepared through the exfoliation–reduction was highly active and selective for oxidation of n-butane." @default.
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• W2006603728 date "2003-02-01" @default.
• W2006603728 modified "2023-09-26" @default.
• W2006603728 title "Preparation of catalyst precursors for selective oxidation of n-butane by exfoliation–reduction of VOPO4·2H2O in primary alcohol" @default.
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• W2006603728 doi "https://doi.org/10.1016/s0920-5861(02)00319-x" @default.
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