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- W2006699722 abstract "Abstract High resolution 19 F NMR spectra of rotating polycrystalline solids can be obtained by single pulse excitation with a long delay before acquisition (SPEDA). However, the overall spectral range is influenced by the chemical shift anisotropy which, unlike the situation for protons, might be large for 19 F nuclei. Three typical cases can be distinguished according to the relative magnitudes of the chemical shift anisotropies and homonuclear dipolar interactions. The second-order effect arising from the non-commutability of the chemical shift and homonuclear dipolar interactions is discussed. The linewidths of the central bands and the characteristics of the sidebands are analyzed. It is found that Anderson-Weiss approximation of the memory equation must be modified to explain the sideband phenomena observed." @default.
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- W2006699722 date "1996-09-01" @default.
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- W2006699722 title "19F SPEDA NMR spectra in rotating solids" @default.
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- W2006699722 doi "https://doi.org/10.1016/0009-2614(96)00800-7" @default.
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