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• W2007014516 abstract "The purine nucleoside 2,6-diaminopurine-2′-deoxyriboside is prepared by the direct glycosylation of the 2,6-bis(tetramethylsuccinimide) derivative of the parent purine heterocycle 4 with 2-deoxy-3,5-di-O-(p-toluoyl)-α-d-erythro-pentofuranosyl chloride 5 using the sodium salt method. 2′-Deoxyisoguanosine is prepared from 2,6-diaminopurine by a five-step procedure. The purine heterocycle isoguanine is prepared by selective diazotization of 2,6-diaminopurine and then converted to the N9-trityl derivative to increase solubility. After silylation of the O2-carbonyl with TMSCl, the N6-amino group is protected as the tetramethylsuccinimide (M4SI). The O2-carbonyl is protected as the DPC derivative, and the trityl group is removed. The resulting product is glycosylated in good yield to generate fully protected 2′-deoxyisoguanosine." @default.
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• W2007014516 date "2010-02-10" @default.
• W2007014516 modified "2023-10-16" @default.
• W2007014516 title "Preparation of the 2′-Deoxynucleosides of 2,6-Diaminopurine and Isoguanine by Direct Glycosylation" @default.
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• W2007014516 doi "https://doi.org/10.1021/jo902616s" @default.
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