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- W2007166061 abstract "The asymmetric oxidation (t-BuO2H, Ti(OPr-i)4, DET) of a series of 1,3-dithiolanes was carried out to produce the corresponding S-oxides with high chemical and optical yields. By contrast, the oxidation of 1,3-dithianes and 1,3-oxathiolane prepared from the same carbonyl compounds gave much lower optical yields. The optical resolution of the model ketone, dl-menthone,via a) 1,3-dithiolane formation b) asymmetric S-oxidation c) chromatographic diasteromeric separation d) regeneration of the carbonyl group, (93% optical yield), is described." @default.
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- W2007166061 date "1986-01-01" @default.
- W2007166061 modified "2023-10-09" @default.
- W2007166061 title "Asymmetric oxidation of 1,3-dithiolanes. A route to the optical resolution of carbonyl compounds" @default.
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- W2007166061 doi "https://doi.org/10.1016/s0040-4039(00)85446-5" @default.
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