Matches in SemOpenAlex for { <https://semopenalex.org/work/W2007168704> ?p ?o ?g. }
Showing items 1 to 87 of
87
with 100 items per page.
- W2007168704 endingPage "137" @default.
- W2007168704 startingPage "133" @default.
- W2007168704 abstract "Abstract Octahydro‐1,3,5,7‐tetranitro‐1,3,5,7‐tetrazocine (HMX) is currently one of the most widely used explosives. 1,3,5,7‐Tetraacetyl‐1,3,5,7‐tetraazacyclooctane (TAT) is an attractive precursor for the synthesis of HMX; the nitration of this key precursor results in both high yield and purity under mild condition. TAT can be prepared either by acetylation of 2,6‐diacetyl‐pentamethylenetetramine (DAPT) or by the condensation of ACN and 1,3,5‐trioxane. However, TAT and DAPT are polar compounds, and are difficult to analyze using reverse phase liquid chromatography. Herein, a chromatography method for the direct separation of these polar compounds was developed using hydrophilic interaction chromatography (HILIC) using a Venusil HILIC column, with ACN/water (95/5, v/v) as the mobile phase. The chromatographic analysis and identification of these polar compounds provide valuable information for the optimization of the synthetic process of TAT." @default.
- W2007168704 created "2016-06-24" @default.
- W2007168704 creator A5010301078 @default.
- W2007168704 creator A5015534012 @default.
- W2007168704 creator A5021792400 @default.
- W2007168704 creator A5037166021 @default.
- W2007168704 creator A5040185559 @default.
- W2007168704 creator A5062172104 @default.
- W2007168704 creator A5067872317 @default.
- W2007168704 creator A5073818261 @default.
- W2007168704 creator A5079093665 @default.
- W2007168704 creator A5084294562 @default.
- W2007168704 date "2014-10-13" @default.
- W2007168704 modified "2023-09-26" @default.
- W2007168704 title "Analysis of Polar Precursors of 1,3,5,7-Tetranitro-1,3,5,7-tetrazocine (HMX) Using Hydrophilic Interaction Chromatography" @default.
- W2007168704 cites W1488509924 @default.
- W2007168704 cites W1980259924 @default.
- W2007168704 cites W2040627487 @default.
- W2007168704 cites W2107176505 @default.
- W2007168704 cites W2167757636 @default.
- W2007168704 cites W2170576635 @default.
- W2007168704 cites W2322035220 @default.
- W2007168704 cites W2330343208 @default.
- W2007168704 doi "https://doi.org/10.1002/prep.201400070" @default.
- W2007168704 hasPublicationYear "2014" @default.
- W2007168704 type Work @default.
- W2007168704 sameAs 2007168704 @default.
- W2007168704 citedByCount "1" @default.
- W2007168704 countsByYear W20071687042023 @default.
- W2007168704 crossrefType "journal-article" @default.
- W2007168704 hasAuthorship W2007168704A5010301078 @default.
- W2007168704 hasAuthorship W2007168704A5015534012 @default.
- W2007168704 hasAuthorship W2007168704A5021792400 @default.
- W2007168704 hasAuthorship W2007168704A5037166021 @default.
- W2007168704 hasAuthorship W2007168704A5040185559 @default.
- W2007168704 hasAuthorship W2007168704A5062172104 @default.
- W2007168704 hasAuthorship W2007168704A5067872317 @default.
- W2007168704 hasAuthorship W2007168704A5073818261 @default.
- W2007168704 hasAuthorship W2007168704A5079093665 @default.
- W2007168704 hasAuthorship W2007168704A5084294562 @default.
- W2007168704 hasConcept C116817701 @default.
- W2007168704 hasConcept C121332964 @default.
- W2007168704 hasConcept C1276947 @default.
- W2007168704 hasConcept C134121241 @default.
- W2007168704 hasConcept C178790620 @default.
- W2007168704 hasConcept C179998833 @default.
- W2007168704 hasConcept C185592680 @default.
- W2007168704 hasConcept C191897082 @default.
- W2007168704 hasConcept C192562407 @default.
- W2007168704 hasConcept C29705727 @default.
- W2007168704 hasConcept C32909587 @default.
- W2007168704 hasConcept C43617362 @default.
- W2007168704 hasConcept C61978335 @default.
- W2007168704 hasConceptScore W2007168704C116817701 @default.
- W2007168704 hasConceptScore W2007168704C121332964 @default.
- W2007168704 hasConceptScore W2007168704C1276947 @default.
- W2007168704 hasConceptScore W2007168704C134121241 @default.
- W2007168704 hasConceptScore W2007168704C178790620 @default.
- W2007168704 hasConceptScore W2007168704C179998833 @default.
- W2007168704 hasConceptScore W2007168704C185592680 @default.
- W2007168704 hasConceptScore W2007168704C191897082 @default.
- W2007168704 hasConceptScore W2007168704C192562407 @default.
- W2007168704 hasConceptScore W2007168704C29705727 @default.
- W2007168704 hasConceptScore W2007168704C32909587 @default.
- W2007168704 hasConceptScore W2007168704C43617362 @default.
- W2007168704 hasConceptScore W2007168704C61978335 @default.
- W2007168704 hasIssue "1" @default.
- W2007168704 hasLocation W20071687041 @default.
- W2007168704 hasOpenAccess W2007168704 @default.
- W2007168704 hasPrimaryLocation W20071687041 @default.
- W2007168704 hasRelatedWork W1991972021 @default.
- W2007168704 hasRelatedWork W2068118433 @default.
- W2007168704 hasRelatedWork W2188246972 @default.
- W2007168704 hasRelatedWork W2377589434 @default.
- W2007168704 hasRelatedWork W2571272986 @default.
- W2007168704 hasRelatedWork W2785946134 @default.
- W2007168704 hasRelatedWork W2970598548 @default.
- W2007168704 hasRelatedWork W4285222818 @default.
- W2007168704 hasRelatedWork W2460880973 @default.
- W2007168704 hasRelatedWork W2487151011 @default.
- W2007168704 hasVolume "40" @default.
- W2007168704 isParatext "false" @default.
- W2007168704 isRetracted "false" @default.
- W2007168704 magId "2007168704" @default.
- W2007168704 workType "article" @default.