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- W2007194865 abstract "Many explorations of transition metal (M)-L system under solvothermal condition, have led to the syntheses of two new 4-heterocyclic acylpyrazolone complexes [Co(L)2(CH3OH)2] (HL = 1-phenyl-3-methyl-4-(2-furoyl)-5-pyrazolone) (1) and [Cr(L)3] (2). Single-crystal X-ray analyses reveal that crystal structures of compound 1 and 2 are respectively orthorhombic, Pbca, a = 15.0378(6) Å, b = 9.8405(4) Å, c = 20.7321(8) Å, V = 3067.9(2) Å3, Z = 8 and triclinic, P-1, a = 10.7966(18) Å, b = 13.023(2) Å, c = 15.520(3) Å, α = 73.011(4)°, β = 84.884(4)°, γ = 70.267(4)°, V = 1964.3(6) Å3, Z = 2. Complex 1 has a two-dimensional (2D) network structure that is formed by O–H···N H-bonding interactions. Complex 2 makes a one-dimensional (1D) zigzag chain structure by intermolecular π···π interactions, which is further interlinked via C–H···N H-bonding interactions to generate a 2D sheet, and then a three-dimensional (3D) supramolecular network structure is further linked by intermolecular C–H···π interactions. (© 2009 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim)" @default.
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- W2007194865 date "2009-06-01" @default.
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- W2007194865 title "Solvothermal syntheses and crystal structures of two 4-heterocyclic acylpyrazolone complexes" @default.
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- W2007194865 doi "https://doi.org/10.1002/crat.200800552" @default.
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