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• W2007226100 endingPage "167" @default.
• W2007226100 startingPage "155" @default.
• W2007226100 abstract "The macrocyclic pentolide 1, hexolide 2, and heptolide 3 constitute ca. 80% of the oligomers formed in ca. 50% yield from enantiomerically pure 3-hydroxybutanoic acid under Yamaguchi's macrolactonization conditions. The FAB mass spectra of the MH+, M Na+, and MCs+ are reported (Figs. 2, 3, 5, and 6). No cyclic tetramer is detected. The 1H-NMR spectra of the cyclic oligomers, of the monomer, and of the polymer (PHB) are very similar (Fig. 4). Directed synthesis of the open-chain dimer and tetramer of 3-hydroxybutanoic acid and attempted cyclization do not lead to the isolation of the cyclic tetramer." @default.
• W2007226100 created "2016-06-24" @default.
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• W2007226100 date "1988-02-03" @default.
• W2007226100 modified "2023-10-18" @default.
• W2007226100 title "High-Yield Synthesis of 20-, 24-, and 28-Membered Macropentolide, -hexolide, and -heptolide, Respectively, from (<i>R</i>)- or (<i>S</i>)-3-hydroxybutanoic acid under<i>Yamaguchi</i>'s macrolactonization conditions" @default.
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• W2007226100 doi "https://doi.org/10.1002/hlca.19880710119" @default.
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