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• W2007232200 abstract "We present the first application of switched angle spinning (SAS) to correlate the first-order dipolar spectrum of a liquid crystalline sample with the isotropic magic angle spinning (MAS) spectrum in a two-dimensional experiment. In this experiment we are able to select the degree of dipolar couplings introduced via mechanical manipulations of the liquid crystal director in a single oriented sample. The (19)F SAS-COSY correlation of iodotrifluoroethylene, an AMX spin system, dissolved in the nematic liquid crystal 4-octylphenyl-2-chloro-4-(4-heptylbenzoyloxy)-benzoate provides assignment of both the J and dipolar couplings in a single experiment. This work demonstrates the use of oriented samples and sample spinning to resolve homonuclear dipolar couplings using isotropic chemical shifts." @default.
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• W2007232200 date "2002-07-01" @default.
• W2007232200 modified "2023-10-16" @default.
• W2007232200 title "Two-Dimensional NMR Correlations of Liquid Crystals Using Switched Angle Spinning" @default.
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• W2007232200 doi "https://doi.org/10.1006/jmre.2002.2571" @default.
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