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- W2007236010 abstract "The unsaturated cluster Os3(CO)8(Ph2PCH2P(Ph)C6H4)(μ-H) (1) reacts with CH2N2 at −10 to 25 °C to give two novel compounds Os3(CO)7(μ3-CN2)(μ-dppm)(μ-H)2 (2) and Os3(CO)7(μ3-CCO2H)(μ-dppm)(μ-H)3 (3) characterized by single-crystal X-ray crystallography. Compound 2 is converted to 3 in almost quantitative yield by reaction with CO (atmospheric pressure) and trace H2O. The reaction of 2 with molecular hydrogen at atmospheric pressure at 80 °C yields Os3(CO)8(μ-dppm)(μ-H)2 (4) and Os3(CO)10(μ-dppm) (5)." @default.
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- W2007236010 date "2000-11-22" @default.
- W2007236010 modified "2023-10-12" @default.
- W2007236010 title "Carboxylation of a μ<sub>3</sub>-Diazo Methylidyne Triosmium Cluster" @default.
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- W2007236010 doi "https://doi.org/10.1021/om000322b" @default.
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