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- W2007374654 abstract "Die Synthese von fünf spezifisch mit 14C markierten Terphenylen wird beschrieben. Brombenzol-4-14C und p-Dibrombenzol-1-14C wurden aus Anilin-1-14C hergestellt. Aus Brornbenzol-4-14C konnte durch Umsetzung mit Butyllithium und 1- Phenylcyclohexanon-2 und 1-Phenylcyclohexanon-4 und anschließende Dehydrierung o- und p-Terphenyl-4-14C bereitet werden. p-Dibrombenzol-1-14C ergab durch doppelte Umsetzung mit Cyclohexanon p-Terphenyl-1′-14C. Entsprechend lieferte p- Dibrombenzol- U14C p-Terphenyl-(1′, 2′, 3′, 4′, 5 ′, 6′)-14C. Aus Cyclohexanon-1-14C konnte über Phenylcyclohexanon und folgende Reaktion mit Phenylmagnesiumbromid o-Terphenyl-1-′14C erhalten werden. The synthesis of five specifically 14C labelled terphenyls is described. Bromobenzene-4-14C and p-dibromobenzene-1-14C was prepared from anilin-1-14C. Bromobenzene-4-14C was reacted with butyllithium and 1-phenylcyclohexanon-2 and 1-phenylcyclohexanon-4, respectively, yielding o-and p-terphenyl-4-14C after dehydrogenation. p-Terphenyl-1′-14C was prepared from p-dibromobenzene-1-14C by a double reaction with cyclohexanon. p-Terphenyl-(1′, 2′, 3′, 4′, 5′, 6′)-14C was obtained in the same way from p-dibromobenzene- U-14C. o-Terphenyl-1′ -14C was synthesized from cyclohexanon-1-14C via phenylcyclohexanon and subsequent reaction with phenylmagnesiumbromide." @default.
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- W2007374654 date "1968-01-01" @default.
- W2007374654 modified "2023-09-27" @default.
- W2007374654 title "Zur Synthese14C-markierter Terphenyle" @default.
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- W2007374654 doi "https://doi.org/10.1002/jlcr.2590040112" @default.
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