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• W2007472612 abstract "Abstract The Hg‐substituted type‐I clathrates A 8 Hg 3+ x Ge 43– x (A = K, Rb) were obtained by solid‐state reactions from the corresponding Zintl phases A 4 Ge 9 and Hg or HgO. The crystal structures of the compounds were determined by single‐crystal and powder X‐ray diffraction methods. They crystallize in the space group Pm $bar {3}$ n , with a = 10.849(1) Å and x = 0.19(5) for K 8 Hg 3+ x Ge 43– x ( 1 ) and a = 10.875(1) Å and x = 0.03(7) for Rb 8 Hg 3+ x Ge 43– x ( 2 ). Specific atomic positions (6 c site) of the Ge framework are partially substituted by Hg atoms, whereas the alkali‐metal atoms reside at the center of the cavities. Both compounds exceed the electron‐counting rule for Zintl phases. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2008)" @default.
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• W2007472612 date "2008-10-01" @default.
• W2007472612 modified "2023-10-17" @default.
• W2007472612 title "A₄Ge₉ (A = K, Rb) as Precursors for Hg‐Substituted Clathrate‐I Synthesis: Crystal Structure of A₈Hg₃Ge₄₃" @default.
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• W2007472612 doi "https://doi.org/10.1002/ejic.200800631" @default.
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