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- W2007495810 abstract "A method for the determination of three tetracyclines (viz. tetracycline, oxytetracycline and doxycycline) is proposed. The method uses a flow manifold coupled on-line to a capillary electrophoresis (CE) system. The tetracyclines are preconcentrated on a STRATA-X solid-phase minicolumn inserted in the manifold. This provides an average recovery of tetracyclines of 92% from spiked water samples. The proposed method allows the resolution of mixtures of tetracyclines at concentrations ranging from 7 to 45 g l−1 and has a limit of detection of 2 g l−1. Under optimal conditions, recoveries range from 99 to 106% and the precision is better than 7.5%. Based on the results, the method is a highly efficient choice for the separation and determination of tetracyclines in surface water samples." @default.
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- W2007495810 date "2004-07-01" @default.
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- W2007495810 title "Rapid determination of trace levels of tetracyclines in surface water using a continuous flow manifold coupled to a capillary electrophoresis system" @default.
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- W2007495810 doi "https://doi.org/10.1016/j.aca.2004.04.050" @default.
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