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• W2007527168 abstract "The conventional method for obtaining transient rheological data on short glass fiber-filled polymeric fluids is to use the parallel disk (PP) geometry in a rotational rheometer. Using the PP geometry large transient stress overshoot behavior was observed during the startup of flow measurements on a 30 wt % short glass fiber-filled polybutylene terephthalate. A contributing factor to this behavior is believed to be induced fiber collisions caused by the inhomogeneous velocity field (radial varying velocity gradient). A novel approach was taken in which a “donut” shaped sample was used in a cone-and-plate device (CP-D) to maintain a sufficient gap to fiber length ratio. The magnitude of the first normal stress difference was reduced by 70%, and the time to reach steady state was reduced by 100 strain units. The Lipscomb model coupled with the Folgar–Tucker model for the evolution of fiber orientation was fit to the stress growth behavior measured using both the PP geometry and CP-D resulting in different parameters. In addition, the fitted model parameters were found to depend on the initial fiber orientation. It is believed that the CP-D allows for an accurate determination of the stress growth behavior and eventually will allow one to obtain unambiguous model parameters." @default.
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• W2007527168 date "2009-09-01" @default.
• W2007527168 modified "2023-10-16" @default.
• W2007527168 title "Obtaining reliable transient rheological data on concentrated short fiber suspensions using a rotational rheometer" @default.
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• W2007527168 doi "https://doi.org/10.1122/1.3177348" @default.
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