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- W2007573796 abstract "Preparation and Reactions of (η51-Pentamethylcyclopentadienyl)1- and (η51-Ethyltetramethylcyclopentadienyl)titanium Trifluoride[1] Compound Cp*TiCl3 (1, Cp*η51-Me5C5) reacts with an excess of AsF3 to yield the crystalline complex [Cp*TiF3]2·2 AsF3 (2). AsF3 can be removed from 2 in vacuo to give Cp*TiF3 (3). Complex (η51-EtMe4C5)TiCl3 (4) is converted by an excess of AsF3 to (η51-EtMe4C5)TiF3 (5). Compound 3 reacts with a lithium 1,3-diketonate to form the hexacoordinated complex (6) and with a lithium benzamidinate to yield pentacoordinated Cp*TiF2[(Me3SiN)2 C-C6H4OMe-(4)] (7): The reaction of 3 with Ph3PNSiMe3 and C2H2(Ph2PNSiMe3)2 leads to Cp*TiF2NPPh3 (8) and (Cp*TiF2NPPh2)2C2H2 (9), respectively. X-Ray structure analyses of compounds 2 and 5–9 have been performed." @default.
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- W2007573796 title "Synthese und Reaktionen von (η <sup>5</sup> 1‐Pentamethylcyclopentadienyl)1‐ und (η <sup>5</sup> 1‐Ethyltetramethylcyclopentadienyl)titantrifluorid" @default.
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- W2007573796 doi "https://doi.org/10.1002/cber.19931260410" @default.
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