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• W2007610930 abstract "Differential Scanning Calorimetry (DSC) measurements were performed on a series of ethylene-vinyl chloride copolymers (E-V) prepared via reductive dechlorination of poly(vinyl chloride) with tributyltin hydride. The copolymers were identical in chain length and branching distribution; differing only in comonomer content, sequence distribution, and stereoregularity of adjacent —V— units. Extrapolation of glass transition temperatures, Tg, measured for our E-V copolymers to pure polyethylene (PE) predicted a Tg = −85 ± 10°C for amorphous PE. E-V copolymers with greater than 60 mol percent —E— units exhibited melting endotherms from 20 to 128°C and degrees of crystallinity from 12 to 63 percent. The melting point depressions observed for our E-V copolymers were in agreement with Flory's theory, if the CH2CH2 moiety is considered to be the crystallizable unit and the moiety is assumed to prevent the CH2CH2 units attached on either side from being incorporated into the crystal. In general, the E-V copolymer blends with PE were incompatible, while those with PVC were compatible only for E-V copolymers with high V contents (>80 mol percent). Blends of the amorphous E-V copolymers were found compatible if their V contents differed by less than 15 mol percent, while blends where one or both E-V copolymers are crystalline were found to be incompatible. The properties of these copolymers will be discussed in terms of their microstructure." @default.
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• W2007610930 date "1986-09-01" @default.
• W2007610930 modified "2023-10-16" @default.
• W2007610930 title "Thermal transitions of ethylene-vinyl chloride copolymers and their blends" @default.
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• W2007610930 doi "https://doi.org/10.1002/vnl.730080303" @default.
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