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• W2008135938 abstract "Rectangular single crystals of amylose complexed with n-butanol or n-pentanol were prepared by adding these precipitants to metastable aqueous solutions of amylose. The crystals were analysed by electron and X-ray diffraction. It was confirmed that the crystals have an orthorhombic P212121 symmetry with cell parameters: a=2.74 nm, b=2.65 nm and c (chain axis)=0.8 nm. Within the unit cell, the amylose chains were organized in antiparallel pairs of parallel 65 amylose helices with four molecules of precipitant located between the helices and occupying about 10% of the cell volume. Upon desolvation, the crystals were invariably converted to the hexagonal close-packed VH amylose. The crystals could also be swollen in a series of solvents or solvent mixtures without losing their single crystal characteristics. Such treatments retained the orthorhombic symmetry but resulted in an expansion of their a and b cell parameters while c remained constant at 0.8 nm." @default.
• W2008135938 created "2016-06-24" @default.
• W2008135938 creator A5042394568 @default.
• W2008135938 creator A5054435498 @default.
• W2008135938 date "1994-01-01" @default.
• W2008135938 modified "2023-10-16" @default.
• W2008135938 title "Single crystals of V amylose complexed with n-butanol or n-pentanol: structural features and properties" @default.
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• W2008135938 doi "https://doi.org/10.1016/0141-8130(94)90052-3" @default.
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