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- W2008314492 abstract "Abstract The tryptophan content of nine samples of food and feedstuffs was determined using two procedures differing mainly by the hydrolysing agent. For a given smaple hydrolyses were conducted at the same time and in the same autoclave at 125°C for 16 h after a purging of the apparatus at 100°C for 5 min. Ba(OH) 2 hydrolysis yielded the highest values for tryptophan. As for NaOH hydrolysates, the tryptophan recovery evaluated from data obtained with Ba(OH) 2 hydrolysates and taken as reference varied from 74·5 to 98·2% with a mean of 88·8%. These values are identical to those reported in literature for recovery of tryptophan added to samples prior to their autoclaving in Ba(OH) 2 on NaOH but without purging at 100°C. The tryptophan recovery corrected from losses of added 5-methyltryptophan varied from 95·3 to 106·8% with a mean of 102·3%. The efficiency of autoclave purging at 100°C for the quantitative recovery of tryptophan from Ba(OH) 2 hydrolyses would be due to a thorough deoxygenation of medium through boiling." @default.
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- W2008314492 date "1994-01-01" @default.
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- W2008314492 title "Determination of tryptophan in feedstuffs: comparison of sodium hydroxide and barium hydroxide as hydrolysis agents" @default.
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- W2008314492 doi "https://doi.org/10.1016/0308-8146(94)90238-0" @default.
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