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- W2008388622 abstract "2,4-O-Benzylidene-D-threose (1) was treated with the Grignard reagent obtained from n-octyl bromide to afford the epimeric tetrol derivatives 3a, b. Regioselective 2-O-mesylation and subsequent azido group introduction furnished azidophytosphingosine derivatives 5a, b. Ensuing 4-O-mesylation, acidcatalyzed benzylidene group removal and then treatment with NaH as a base provided preferentially the desired 3,4-epoxide derivatives 8a, b; subsequent azido group reduction with triphenylphosphane/water yielded the target molecules 9a, b possessing D-ribo and L-lyxo configuration, respectively." @default.
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- W2008388622 date "1993-01-21" @default.
- W2008388622 modified "2023-10-16" @default.
- W2008388622 title "Epoxides of Phytosphingosine and Derivatives, Potential Inhibitors of Sphingosine Biosynthesis" @default.
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- W2008388622 doi "https://doi.org/10.1002/jlac.199319930112" @default.
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