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- W2008496638 abstract "Six new silver(I) double salts, namely [Ag13(C2)2(CF3CO2)9(bipy)4(H2O)3] (1), [Ag18(C2)2(C2F5CO2)18(bipyH)4] · 3H2O (2), [Ag6(C2)(CF3CO2)4(bpp)] (3), [Ag6(C2)(C2F5CO2)5(bppH)]n (4), [Ag6(C2)(CF3CO2)5(bppH)]n (5) and [Ag23(C2)4(CF3CO2)15(bpp)6] · H2O (6) (bipy = 4,4′-bipyridine, bpp = bis(4-pyridyl)propane), have been hydrothermally synthesized and structurally characterized. In complex 1, the building units [Ag24(C2)4(CF3CO2)16(H2O)6] are connected by bipy ligands to form a two-dimensional network, which are further linked into a three-dimensional architecture via argentophilic interactions. Complex 2 is composed of two independent [Ag(bipyH)2]3+cations and a [Ag16(C2)2(C2F5CO2)18]6− cluster, whose core is a (C2)2@Ag16 double cage constructed from edge-sharing of two monocapped square antiprisms. Complex 3 has a two-dimensional architecture generated from bpp-bridged silver(I) columns. The virtually iso-structural complexes 4 and 5 each has a branched-tree architecture. The backbone is composed of fused silver(I) double cages, with C22- species embedded in its stem and an exterior coat comprising anionic perfluorocarboxyate and protonated bpp ligands. Complex 6 exhibits a two-dimensional architecture in which the basic building unit is an unusual silver(I) column composed of four consecutively fused C2@Agn cages." @default.
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- W2008496638 date "2005-06-01" @default.
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- W2008496638 title "4,4′-Bipyridine and bis(4-pyridyl)propane as bridging ligands in the supramolecular assembly of silver(I) polyhedra containing embedded acetylenediide" @default.
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- W2008496638 doi "https://doi.org/10.1016/j.poly.2005.03.005" @default.
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