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- W2008650054 abstract "The preparation of TiSi2 single crystals by chemical transport in the presence of halogens is studied. It is shown that the tetrahalides formed during the interaction of TiSi2 with halogens, and above all the tetrahalides of titanium, TiX4, are the transporting agents. The gas phase composition is complex in all cases, but according to thermodynamic analysis silicon should be transported in the form of a dihalide, SiX2, whereas titanium transport should occur through TiX3 and TiX2, the contribution of the latter increasing in the sequence chlorine → bromine → iodine. Single crystals of TiSi2 are obtained in the presence of the three halogens, but transport with chlorine is found to be the most efficient. The conditions for the preparation of TiSi2 single crystals in the form of needles, polyhedra or plates with maximum dimensions of 10 mm, 4 mm and 5 mm, respectively, and a composition close to the stoichiometric are established." @default.
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- W2008650054 date "1986-03-01" @default.
- W2008650054 modified "2023-09-27" @default.
- W2008650054 title "Preparation of titanium disilicide single crystals by chemical vapour transport with halogens" @default.
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- W2008650054 doi "https://doi.org/10.1016/0022-5088(86)90061-5" @default.
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