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- W2009411633 abstract "A simple and direct approach was developed for thermochemolytic analysis of a wide range of biomolecules present in plant materials using an injection port of a gas chromatograph/mass spectrometer (GC/MS) and a novel solids injector consisting of a coiled stainless steel wire placed inside a modified needle syringe. Optimum thermochemolysis (or Thermally Assisted Hydrolysis/Methylation) was achieved by using a suitable methanolic solution of trimethylsulfonium hydroxide (TMSH) or tetramethylammonium hydroxide (TMAH) with an injection port temperature of 350 °C. Intact, methylated flavonoids, saccharides, phenolic and fatty acids, lignin dimers and diterpene resin acids were identified. Samples include tea leaves, hemicelluloses, lignin isolates and herbal medicines. Unexpected chromatographic results using TMAH reagent revealed the presence of intact methylated trisaccharides (658 Da) and structurally informative dimer lignin markers." @default.
- W2009411633 created "2016-06-24" @default.
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- W2009411633 date "2009-07-01" @default.
- W2009411633 modified "2023-09-25" @default.
- W2009411633 title "Use of an injection port for thermochemolysis–gas chromatography/mass spectrometry: Rapid profiling of biomaterials" @default.
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- W2009411633 doi "https://doi.org/10.1016/j.chroma.2009.06.014" @default.
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