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- W2009483313 abstract "Abstract A new high yield (75–95%) method—condensation of polyhedral clusters—for synthesis of octahedral rhenium cluster compounds Re 6 X 4 Br 10 and Re 6 X 8 Br 2 (X = S, Se, Te) has been developed using triangular cluster rhenium bromide Re 3 Br 9 and lead or cadmium chalcogenides as starting materials. The phases obtained were characterized by chemical analysis and X-ray powder diffraction method, and the cell unit parameters of compounds were found. The crystal structure of Re 6 Te 4 Br 10 was solved by X-ray single crystal analysis. Crystallographic data: triclinic, space group P 1, a = 9.347(2), b = 9.403(4), c = 13.348(4) A , α = 84.46(3), β = 84.64(2), γ = 82.11(2) °, V = 1152.8(6) A 3 , Z = 2, D x = 6.991 g-cm −3 , R(F) = 0.0378, wR(F 2 ) = 0.0906." @default.
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- W2009483313 title "Synthesis of octahedral rhenium cluster chalcobromides Re6X4Br10 and Re6X8Br2(X = S, Se, Te) by condensation from triangular rhenium bromide Re3Br9" @default.
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- W2009483313 doi "https://doi.org/10.1016/s0025-5408(97)00102-5" @default.
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