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• W2009552170 abstract "Abstract A multi-anvil press was combined with monochromatic synchrotron X-ray radiation to investigate the synthesis, at high-pressure high-temperature conditions, of a recoverable bulk sample of Fe 4 O 5 , from an initial magnetite, Fe 3 O 4 , sample. Angle-dispersive diffraction patterns show that magnetite firstly breaks down, into an assemblage of hematite (Fe 2 O 3 ) + Fe 4 O 5 . By increasing temperature at constant load, hematite disappears progressively by either reduction or by melting, or a combination of both. In the final product only Fe 4 O 5 remains and, in the absence of hematite, can be kept stable and be recovered at ambient conditions. Refinement of the diffraction patterns at standard conditions demonstrate that Fe 4 O 5 has the Sr 2 Tl 2 O 5 -type-structure with space group Cmcm and a = 2.8964(2) Å, b = 9.8225(6) Åand c = 12.5808(7) Å. This structure-type and related members of a homologous series, offer the possibility that the general sequence of AB (2+ n ) X (4+ n ) chemistries could, under certain conditions, be extended to accommodate prevalent oxygen fugacity or, indeed, other ordered stoichiometries through extension of the c axis by the addition of FeO 6 octahedral blocks. This structural series, as in other systems, offers possibilities of hosting charge-transfer, Jahn-Teller and other electronic phenomena − as well as supporting metric distortions. Each of these possibilities is highlighted through illustration and extension to related structure-types, most notably from those of the spinels, post-spinels and post-perovskites." @default.
• W2009552170 created "2016-06-24" @default.
• W2009552170 creator A5034497299 @default.
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• W2009552170 date "2014-04-01" @default.
• W2009552170 modified "2023-10-02" @default.
• W2009552170 title "Synthesis and recovery of bulk Fe₄O₅ from magnetite, Fe₃O₄. A member of a self-similar series of structures for the lower mantle and transition zone" @default.
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• W2009552170 doi "https://doi.org/10.1180/minmag.2014.078.2.09" @default.
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