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- W2009658995 abstract "The synthesis and structural characterization of three silicon diacetylenic heterocyclynes 1,1-diisopropyl-4,5:10,11-dibenzosilacyclotrideca-4,10 diene-2,6,8,12-tetrayne (4), 1,1-dimethyl-4,5:10,11-dibenzosilacyclotrideca-4,10-diene-2,6,8,12-tetrayne (5), and 1-methyl-1-n-octadecyl-4,5:10,11-dibenzosilacyclotrideca-4,10-diene-2,6,8,12-tetrayne (6) are reported. A dimer (7) and a cobalt complex (9) of 4 have also been characterized. Deprotonation of 1,4-di-(o-ethynylphenyl)butadiyne with two equivalents of n-BuLi resulted in the formation of the dianion. Addition of one equivalent of the appropriate dialkyldichlorosilane to a highly diluted THF solution of the dianion resulted in the formation of compounds 4, 5, 6 and 7. These compounds were irradiated and were annealed. Comparisons to related compounds are made." @default.
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- W2009658995 date "1999-04-01" @default.
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- W2009658995 title "Syntheses and crystal structures of strained planar silacyclynes containing a diacetylene unit" @default.
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- W2009658995 doi "https://doi.org/10.1016/s0022-328x(98)01102-4" @default.
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