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• W2009703059 abstract "Low-temperature structural properties of the synthetic mineral libethenite Cu2PO4OH were investigated by single-crystal X-ray diffraction, synchrotron X-ray powder diffraction, specific heat measurements, and Raman spectroscopy. A second-order structural phase transition from the Pnnm symmetry (a=8.0553(8) Å, b=8.3750(9) Å, c=5.8818(6) Å at 180 K) to the P21/n symmetry (a=8.0545(8) Å, b=8.3622(9) Å, c=5.8755(6) Å, β=90.0012(15) at 120 K) was found at 160 K during cooling. At 120 K, the monoclinic angle is 90.0012(15) from single crystal X-ray data vs 90.083(1) from powder X-ray diffraction data. The P21/n–to–Pnnm transition may be a general feature of the adamite-type compounds, M2XO4OH." @default.
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• W2009703059 date "2011-11-01" @default.
• W2009703059 modified "2023-10-05" @default.
• W2009703059 title "Low-temperature structural phase transition in synthetic libethenite Cu2PO4OH" @default.
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• W2009703059 doi "https://doi.org/10.1016/j.jssc.2011.09.026" @default.
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