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- W2009743087 abstract "Abstract The compounds α- and β-SbIIISbV(P2O7)2 were obtained by heating at 923 K (α-type) or 773 K (β-type) a mixture of Sb2O5,nH2O with an excess of NH4H2PO4. α-SbIIISbV(P2O7)2 crystallizes in the monoclinic system, space group P2 1 c with a = 8.088(1) A, b = 16.015(3) A, c = 8.135(5) A, β = 90.17(2)°, Z = 4. The β-type crystallizes in the orthorhombic system, space group Pna21, with a = 8.018(1) A, b = 16.134(3) A, c = 8.029(5) A, Z = 4. Both crystal structures were determined from reflections collected on a Nonius CAD4 automatic diffractometer with Mo K α radiation. The final R index and weighted Rw index are 0.041 and 0.050, respectively, for α- and 0.041 and 0.052, respectively, for β-SbIIISbV(P2O7)2. Both structures are built up from corner-shared SbIIIO6 or SbVO6 octahedra and P2O7 groups. Each P2O7 group shares its six vertices with six different SbO6 octahedra and each octahedron is connected with six P2O7 groups thus leading to two different three-dimensional frameworks. Nevertheless, both structures are closely related to that of the zirconium diphosphate ZrP2O7." @default.
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- W2009743087 date "1988-08-01" @default.
- W2009743087 modified "2023-10-04" @default.
- W2009743087 title "New mixed-valence antimony phosphates: α- and β-SbIIISbV(P2O7)2" @default.
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- W2009743087 doi "https://doi.org/10.1016/0022-4596(88)90161-2" @default.
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