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• W2009811972 abstract "Uranyl nitrate reacts with citric (H4cit) or d-(−)-citramalic (H3citml) acids under mild hydrothermal conditions and in the presence of diamines to give different complexes which are all characterized by the presence of 2:2 uranyl/polycarboxylate dianionic dimers or of polymeric chains based on the same dimeric motif. Each uranium ion is chelated by the two ligands through the alkoxide and the α- or β-carboxylate groups, the second β-carboxylic group in citrate being uncoordinated. The uranium coordination sphere is completed by either a water molecule or the β-carboxylate group of a neighboring unit, thus giving zero- or one-dimensional assemblages, respectively. The evidence for [UO2(Hcit)]2 dimers in the solid state confirms previous results from potentiometric and EXAFS measurements on solutions. Depending on the diamine used (DABCO, 2,2‘- and 4,4‘-bipyridine, [2.2.2]cryptand) and its ability to form divergent hydrogen bonds or not, different uranyl/polycarboxylate topologies are obtained, thus evidencing template effects, and extended hydrogen bonding gives two- or three-dimensional assemblages. These results, together with those previously obtained with NaOH as a base, add to the knowledge of the uranyl/citrate system, which is much investigated for its environmental relevance." @default.
• W2009811972 created "2016-06-24" @default.
• W2009811972 creator A5063941923 @default.
• W2009811972 date "2007-02-13" @default.
• W2009811972 modified "2023-09-30" @default.
• W2009811972 title "Uranyl Ion Complexation by Citric and Citramalic Acids in the Presence of Diamines" @default.
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• W2009811972 doi "https://doi.org/10.1021/ic061772k" @default.
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