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• W2009866586 abstract "Abstract The hydrous calcium carbonate mineral ikaite (CaCO 3 .6H 2 O) forms in nature at low temperature in carbonate- and Ca-rich waters. Ikaite crystallizes in the spacegroup C2/ c , and consists of CaCO 3 .6H 2 O units with Ca ions coordinated by eight oxygens, six from H 2 O and two from the carbonate group. Hydrogen bonding links CaCO 3 .6H 2 O moieties to form the crystal structure. We have used synchrotron X-ray powder diffraction at T = 243 K to refine the monoclinic structure of ikaite, and have measured unit-cell parameters of ikaite between T = 114 K and T = 293 K. Anisotropic thermal expansion in ikaite is evident, with the smallest relative increase occurring along the b direction parallel to 2-fold axes. The contribution of hydrogen bonding to thermal expansion is assessed by comparison of our data with previously published data for deuterated ikaite, ice and gypsum. Ikaite exhibits a coefficient of volume expansion intermediate between that of ice (Ih) and of deuterated gypsum (CaSO 4 .2D 2 O) between T = 114 K and T = 293 K." @default.
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• W2009866586 date "2004-02-01" @default.
• W2009866586 modified "2023-10-18" @default.
• W2009866586 title "The structure and thermal expansion behaviour of ikaite, CaCO₃. 6H₂O, from <i>T</i> = 114 to <i>T</i> = 293 K" @default.
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• W2009866586 doi "https://doi.org/10.1180/0026461046810176" @default.
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