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• W2009898688 abstract "Three new interesting discrete dinuclear metallocyclic complexes, namely, {[Pd 2 ( 1 ) 4 ](NO 3 ) 4 ·2DMSO·2H 2 O} n ( 4 ), [Pd 2 ( 2 ) 2 Br 4 ] n ( 5 ), and {[Pd 2 ( 3 ) 2 Cl 4 ]·4DMSO} n ( 6 ) have been successfully synthesized by the reaction of flexible exo-bidentate imidazole-containing ligands 1,3-bis(imidazol-1-ylmethyl)benzene ( 1 ), 1,3-bis(imidazol-1-ylmethyl)-5-methylbenzene ( 2 ), and 2,6-bis(imidazol-1-ylmethyl)-4- tert -butylphenol ( 3 ) with corresponding palladium salts. All these complexes were characterized by NMR spectroscopy in combination with elemental analysis, powder X-ray diffraction (PXRD), single-crystal X-ray diffraction, and thermal gravimetric analysis (TGA), respectively. Though all three complexes involve the similar supramolecular building blocks [2+2] metallocyclic units, under the inducement effect of the organic ligands, compounds 4 – 6 exhibit delicate geometric diversification of the resulting high-dimensional inorganic–organic supramolecular assemblies (e.g., [4+2] lantern-like cage structure, 1D channel, and 2D undulating framework, respectively). Furthermore, these results demonstrate that the secondary interactions such as intermolecular π⋯π stacking interactions and hydrogen bonds could play important roles in the aspect of linking low-dimensional entities into high-dimensional supramolecular frameworks." @default.
• W2009898688 created "2016-06-24" @default.
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• W2009898688 date "2013-09-01" @default.
• W2009898688 modified "2023-09-26" @default.
• W2009898688 title "Distinct structures of inorganic–organic supramolecular assemblies based on discrete metallocyclic complexes incorporating flexible imidazole ligands: Syntheses, crystal structures and properties" @default.
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• W2009898688 doi "https://doi.org/10.1016/j.ica.2013.07.014" @default.
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