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- W2010011859 abstract "Abstract Three new compounds, Cs 4 (SeO 4 )(HSeO 4 ) 2 (H 3 PO 4 ) (I), Cs 3 (HSeO 4 ) 2 (H 2 PO 4 ) (II), and Cs 5 (HSeO 4 ) 3 (H 2 PO 4 ) 2 (III), were synthesized from water solutions of CsHSeO 4 /CsH 2 PO 4 . According to X-ray single-crystal analysis, the compounds have the following crystal data: I, monoclinic, space group P 2 1 , a = 5.915(1) A, b = 13.797(3) A, c =11.828(2) A, β =95.11(3)°, V =961.4 A 3 , Z = 2, R 1 = 0.0384; II, monoclinic, space group P 2 1 / n , a =20.281(8) A, b =8.039(4) A, c = 9.160(4) A, β =99.96(4)°, V =1470.9 A 3 , Z =4, R 1 = 0.0580; III, monoclinic, space group C 2/ c , a =33.855(8) A, b =7.978(2) A, c =9.217(2) A, β =101.00(2)°, V =2443.7 A 3 , Z =4, R 1 = 0.0519. All three compounds have in common a coordination number of cesium of 10 or 10+1, with Cs–O distances from 2.9 to 3.8 A. P and Se atoms form the individual tetrahedra with different H-bonding connectivity in structures I–III. PO 4 –SeO 4 layers with attached SeO 4 groups are present in I. Structure II contains a three-dimensional hydrogen bonding network, whereas structure III is characterized by PO 4 –SeO 4 bands to which additional SeO 4 tetrahedra are attached." @default.
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- W2010011859 date "1998-12-01" @default.
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- W2010011859 title "New Cesium Hydrogen Selenate Phosphates: Synthesis and Crystal Structures" @default.
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- W2010011859 doi "https://doi.org/10.1006/jssc.1998.7921" @default.
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