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- W2010034741 abstract "A synthesis of (2S,3S,7S)-3,7-dimethylpentadecan-2-yl acetate (2) and propionate (3) is described. (2S)-2-Methyldecan-1-yl lithium (5) was reacted with (3S,4S)-3,4-dimethyl-γ-butyrolactone (6) to yield the ketoalcohol 19 which upon Huang-Minlon reduction furnished (2S,3S,7S)-3,7-dimethylpentadecan-2-ol (1). Acylations gave the esters 2 and 3. The (2S)-2-methyldecan-1-yl lithium was obtained via asymmetric synthesis. The chiral lactone 6 was obtained from (2S,3S)-trans-2,3-epoxybutane and dimethyl malonate." @default.
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- W2010034741 date "1981-01-01" @default.
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- W2010034741 title "Chiral synthesis of (2s,3s,7s)-3,7-dimethylpentadecan-2-yl acetate and propionate, potential sex pheromone components of the pine saw-fly neodiprion sertifer (geoff.)" @default.
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- W2010034741 doi "https://doi.org/10.1016/s0040-4020(01)97980-3" @default.
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