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• W2010090596 abstract "A series of syntheses in the HF–ZrO 2 –P 2 O 5 –pyridine–H 2 O system have been performed in an attempt to synthesize novel materials with open zirconium phosphate framework structures. One of the resulting products, designated ZrPOF–pyr (∣(C 5 H 6 N) 4 (H 2 O) 2 ∣ [Zr 12 P 16 O 60 (OH) 4 F 8 ]), has been characterized by XRD, SEM and TG-DTA, and its crystal structure determined from powder diffraction data using direct methods ( Pnnm , a = 19.1595(2) Å, b = 15.1428(1) Å, c = 6.61804(6) Å). The framework structure, consisting of corner sharing ZrO 6 , ZrO 5 F, ZrO 4 F 2 octahedra and PO 4 and PO 3 OH tetrahedra, proved to be identical to that of ∣(C 5 H 16 N 2 ) 2 (H 2 O) 6 ∣ [Zr 12 P 16 O 60 (OH) 4 F 8 ], which had been reported previously. In both structures, the terminal P–OH group is disordered. The non-framework species (pyridinium ion and water molecule) could be located in the channels of the framework. Structure solution was also performed using a charge-flipping algorithm, which makes no symmetry assumptions, to verify that the P–OH disorder is inherent to the material and not a result of an incorrectly assumed space group. The phase is thermally stable to 450 °C, but transforms to another phase at higher temperatures." @default.
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• W2010090596 date "2007-08-01" @default.
• W2010090596 modified "2023-09-27" @default.
• W2010090596 title "Synthesis, characterization and crystal structure analysis of an open-framework zirconium phosphate" @default.
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• W2010090596 doi "https://doi.org/10.1016/j.micromeso.2007.02.003" @default.
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