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- W2010163061 abstract "An optimisation study based upon experimental data obtained from multivariate statistical experimental design and modelling for the haloform reaction used for synthesis of 3,4-dimethoxybenzoic acid from 3,4-dimethoxy acetophenone is reported. It is shown how the different controllable process variables influence both the yield of 3,4-dimethoxybenzoic acid and the formation of the side product 2-chloro-4,5-dimethoxybenzoic acid. Two predictive multivariate models are derived and used to predict optimal conditions for the oxidation process. Using these models, a yield of 90% (from approximately 60%) of desired product is achieved. Moreover, the model describing the formation of the side-product can in fact also be applied to optimise a procedure for obtaining 2-chloro-4,5-dimethoxybenzoic acid in substantial quantities. One experiment showed that the side-product could be formed in a quantity of >20%." @default.
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- W2010163061 date "1999-08-04" @default.
- W2010163061 modified "2023-09-26" @default.
- W2010163061 title "Fine Chemicals from Lignosulfonates. 2. Synthesis of Veratric Acid from Acetovanillon" @default.
- W2010163061 cites W2005051528 @default.
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- W2010163061 doi "https://doi.org/10.1021/op9900030" @default.
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