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- W2010264908 abstract "This paper demonstrates two simple ways to increase 5-hydroxymethylfurfural (HMF) yield (selectivity) in fructose dehydration with various solid acid catalysts. One is a water removal from the reaction mixture by a mild evacuation at 0.97 × 105 Pa; it increases HMF yield for various catalysts (heteropoly acid, zeolite, and acidic resin). The removal of water suppresses two undesired reactions: the hydrolysis of HMF to levulinic acid and the reaction of partially dehydrated intermediates to condensation products. The other method is a decrease in the particle (bead) size of the resin (Amberlyst-15). The crushed and sieved Amberlyst-15 powder in a size of 0.15–0.053 mm shows 100% HMF yield at high fructose concentration (50 wt.% in DMSO), which is to our knowledge the highest yield to date. Near-infrared spectroscopic characterization of adsorbed water suggests that the enhanced yield can be caused by an improved removal of adsorbed water in a small-size resin particle." @default.
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- W2010264908 date "2009-08-01" @default.
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- W2010264908 title "Enhanced production of hydroxymethylfurfural from fructose with solid acid catalysts by simple water removal methods" @default.
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- W2010264908 doi "https://doi.org/10.1016/j.catcom.2009.06.012" @default.
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