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- W2010315902 abstract "Proton magnetic resonance (1H NMR) was used to study cis-trans isomerization in N-methyl-N-(1-methylthio-2-propenyl)formamide and N-benzyl-N-(1-methylthio-2-propenyl)formamide, two analogs of the thiol form of thiamine. Benzene dilution studies and shift reagent studies were used to make resonance assignments, which indicate that the predominant isomer for each analog has the CC bond trans to the carbonyl oxygen. Shift reagent studies, using Pr(fod)3 in CCl4 or CDCl3, suggest that the reagent may be bonding to both the nitrogen and oxygen atoms of the substrate. For some of the systems studied, varying ρ at constant temperature had the same spectral effect as varying temperature at constant ρ." @default.
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- W2010315902 date "1984-02-01" @default.
- W2010315902 modified "2023-09-25" @default.
- W2010315902 title "1H NMR study ofcis-trans isomerization in two analogs of the thiol form of thiamine" @default.
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- W2010315902 doi "https://doi.org/10.1002/mrc.1270220204" @default.
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