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- W2010354429 abstract "The first total syntheses of O-methylcularicine 9b and sarcocapnine 9c are described together with a new synthesis of cularine 9a using the Ullmann condensation reaction of the appropriate 2′-bromo-8-hydroxy-tetrahydrobenzylisoquinoline formed by phase-transfer alkylation of Reissert compound 2. When this strategy was combined with the lead tetraacetate treatment of the tetrahydrobenzylisoquinoline it yielded 4-hydroxycularines, from which highly oxidized members of the family can be obtained. This is exemplified by the first synthesis of 4-hydroxysarcocapnine 19 and its transformation to the 3,4-dioxoisocularine yagonine 20, rearrangement of which afforded the aristoisocularine aristoyagonine 21." @default.
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- W2010354429 date "1987-03-01" @default.
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- W2010354429 title "Synthetic approaches to cularines. II. Ullmann condensation" @default.
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- W2010354429 doi "https://doi.org/10.1002/jhet.5570240204" @default.
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