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- W2010400116 abstract "Diethylaminosulfur trifluoride (DAST) reacts with dialcohols to give difluorides, sulfite esters or cyclic ethers depending on the number of carbons separating the two alcohol groups. Vicinal and 1,3-diols give large amounts of sulfite ester products while butane-1,4-diol gives almost exclusively the cyclic ether tetrahydrofuran. Terminal dialcohols longer than four carbons give primarily difluoride products. Semiempirical calculations indicate a preference for cyclic intermediates when four or less carbons separate the two alcohol moieties. These cyclic intermediates lead directly to the cyclic ethers and sulfite ester products." @default.
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- W2010400116 date "1995-01-01" @default.
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- W2010400116 title "Reaction of diethylaminosulfur trifluoride with diols" @default.
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- W2010400116 doi "https://doi.org/10.1039/p29950000861" @default.
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