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- W2010406972 abstract "Abstract Carbon-13 and proton NMR spectra have been determined for organothallium (III) derivatives of the types RTlX 2 and R 2 TlX (R (CH 3 ) 3 CCH 2 or (CH 3 ) 3 SiCH 2 ; X Cl, Br or O 2 CCH(CH 3 ) 2 ). The dependence of coupling of 13 C and 1 H to thallium on the number and nature of R groups is discussed in terms of the Fermi contact mechanism for spinspin coupling. The crystal structure of [(CH 3 ) 3 SiCH 2 ] 2 TlCl has been determined. The compound crystallises in the monoclinic space group P 2 1 / n , with a 10.618, b 24.492, c 6.017 A, β 99.76°. The molecule is dimeric with each four-coordinate thallium atom bonded unequally to two bridging chlorine atoms. The CTlC angle is 168°." @default.
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- W2010406972 date "1980-07-01" @default.
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- W2010406972 title "Carbon-13 and proton NMR parameters of neopentyl-and trimethylsilylmethyl-thallium(III) derivatives and the x-ray crystal structure of bis(trimethylsilylmethyl)chlorothallium(III)" @default.
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- W2010406972 doi "https://doi.org/10.1016/s0022-328x(00)86072-6" @default.
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