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- W2010487782 abstract "The phase diagram for the binary system nafcillin sodium-water, was determined using differential scanning calorimetry (DSC) and polarized light microscopy. In the temperature range of −20–30°, three crystalline forms and an amphiphilic liquid crystalline phase were detected. The stable crystalline form of nafcillin sodium (form α) and water exhibit a eutectic mixture containing 28% drug (w/w) at −1°. In more dilute solutions a lower temperature eutectic (−5°) occurs. The composition and form of nafcillin sodium in this eutectic are not known. The form in the −5° eutectic was found to be metastable above 28% concentration and converted to form α. Two other crystalline forms were observed at 9° (form β) and 22° (form γ) at concentrations above 40%. The crystalline forms could not be further characterized due to their transient nature and existence in highly concentrated mixtures. A lamellar mesophase is present near ambient temperature in mixtures containing more than 55% nafcillin sodium. The phase equilibria were highly susceptible to supercooling. Temperature cycling methods were devised which gave reproducible DSC data and allowed construction of the phase diagram." @default.
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- W2010487782 title "Phase Equilibria of Nafcillin Sodium-Water" @default.
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- W2010487782 doi "https://doi.org/10.1002/jps.2600710125" @default.
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