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- W2010520900 endingPage "8350" @default.
- W2010520900 startingPage "8336" @default.
- W2010520900 abstract "Practical EPC-syntheses of δ-substituted-β-keto δ-lactones, subunits of the cochleamycins and macquarimicins, are presented. In consequence Tietze's tandem reaction is employed to combine δ-allyl-β-keto δ-lactone with a hydrindene derivative, the second subunit of these acetogenic antibiotics. Model reactions for the final oxidative radical tandem cyclization reveal that the electrophilic radical cyclizes exclusively in exo-trig fashion. However, with the intended precursor of macquarimicin C allylic hydrogen abstraction thwarted the oxidative radical tandem cyclization." @default.
- W2010520900 created "2016-06-24" @default.
- W2010520900 creator A5024972089 @default.
- W2010520900 creator A5031538161 @default.
- W2010520900 creator A5034757921 @default.
- W2010520900 creator A5054994920 @default.
- W2010520900 creator A5071828228 @default.
- W2010520900 creator A5078438269 @default.
- W2010520900 date "2007-08-01" @default.
- W2010520900 modified "2023-10-09" @default.
- W2010520900 title "Towards EPC-syntheses of the structural class of cochleamycins and macquarimicins. Part 3: EPC-syntheses of the β-keto lactone subunits and first attempts towards the syntheses of the pentacyclic antibiotics of this group" @default.
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